Chaires industrielles - Chaires industrielles

Optimizing mechanical properties of nickel base superalloys by tailoring microstructure – OPALE

Optimizing mechanical properties of nickel base superalloys by tailoring the microstructure of the forged pieces

The French group Safran is among the world leaders in the field of superalloys metallurgy which appeared in the USA in the 40's. This position must be defended, in a highly competitive international context By carrying out research projects on superalloys forming, resulting microstructures and in-service properties (especially for aeronautics), the OPALE chair will educate metallurgists to contribute to the development the French industry and to maintain its competitiveness at the world scale.

Controlling materials to improve the efficiency of turbojet engines

The project aims at improving the mechanical behaviour of polycrystalline Nickel base superalloys, by tailoring the microstructure of as-shaped pieces. Those alloys are used for manufacturing turbojet engine components, due to their excellent mechanical strength at high temperature. Improving the material properties is a necessary condition for increasing the engine temperature and energetic efficiency. The OPALE project is therefore in line with the objectives “Vision 2020” defined by the ACARE.

The OPALE project meets the needs of the Safran group and combines the expertise of the CEMEF (MINES ParisTech, UMR CNRS) on the process-microstructure relationship, and the expertise of the P’ institute (UPR CNRS, ISAE/ENSMA) on the impact of microstructure on the in-service mechanical properties. The chair aims at strengthening and expanding collaborations which already exist between some of the companies of the Safran group and these two research centers. It will help in structuring research on superalloys in Safran, and in establishing long lasting links with the most relevant research labs in the field.
This organization is set up to handle all the topics that will be addressed in the chair to make the metallurgy of tomorrow emerge. The metallurgy of the future will indeed rely on predictive models covering the entire material processing chain as well as its behavior and evolution in service. Such chained models will be developed within the OPALE project.

The OPALE chair aims at a better understanding of metallurgical mechanisms of nickel base superalloys, be they active during processing or during the service life of the component. Various outcomes can be listed : innovative microstructure characterization techniques ; discovery of new mechanisms ; microstructure prediction depending on the thermomechanical route followed (forging and heat treatments) ; fine analyse of the microstructure-properties relationship ; definition of optimal microstructure for a given targetted property ; predictive models for the microstructure of forged components and related properties.

These results will be used by the Sagran group engineers when defining new processing routes, and thus will help Sfarn in maintaining its position within the worldwide competitive scene.
The developped methodologies will be beneficial to address other types of metallic alloys and other application fields in the future.

Results are published in high level scientific journals and are also communicated to the international academic community during conferences. The activity of the OPALE chair is well received by the community, which contributes to the international influence of the French research in the field Metallurgy.
The list of publications and communications is available on-line on the OPALE web site.

The French group Safran is among the world leaders in the field of superalloys metallurgy which appeared in the United States in the 1940s. This position, shared with General Electric, Pratt & Whitney or Rolls-Royce must be defended, especially with regards to the American supremacy. The risk of dilapidation of the French know-how in the field of metallurgy was stressed in a joint report of the Academy of Sciences and Academy of Technology in 2011. At the national scale, metallurgy accounts for 1.5 million jobs and will provide more than 100,000 hirings per year by 2020, with a significant increase in the need for highly qualified categories.
Through the development of projects on superalloys forming, resulting microstructures and in-service properties (especially for aeronautics), the OPALE chair will educate metallurgists who will later on contribute to the development the French industry and to maintain its competitiveness at the world scale in the future.
The project aims at improving the mechanical behaviour of polycrystalline Nickel base superalloys, by tailoring the microstructure of as-shaped pieces. Those alloys are used for manufacturing turbojet engine components, due to their excellent mechanical strength at high temperature. Improving the material properties is a necessary condition for increasing the engine temperature and energetic efficiency. The OPALE project is therefore in line with the objectives “Vision 2020” defined by the ACARE.
The OPALE project meets the needs of the Safran group and combines the expertise of the CEMEF (MINES ParisTech, UMR CNRS) on the process-microstructure relationship, and the expertise of the P’ institute (UPR CNRS, ISAE/ENSMA) on the impact of microstructure on the in-service mechanical properties. The chair aims at strengthening and expanding collaborations which already exist between some of the companies of the Safran group and these two research centers. It will help in structuring research on superalloys in Safran, and in establishing long lasting links with the most relevant research labs in the field.
This organization is set up to handle all the topics that will be addressed in the chair to make the metallurgy of tomorrow emerge. The metallurgy of the future will indeed rely on predictive models covering the entire material processing chain as well as its behavior and evolution in service. Such chained models will be developed within the OPALE project.
The person proposed to be the chair holder, Nathalie Bozzolo, is an experienced scientist who joined the CEMEF recently (2009) to develop activities in that research field in connection with industry. Expert in physical metallurgy, and especially in the analysis of microstructural mechanisms, she is at the junction between the two branches of the project: process-microstructure and microstructure-properties relationships.
The three other involved researchers complete the large competency spectrum needed to achieve that ambitious project: from fine material and properties analysis to process-microstructure and microstructure-properties relationship modelling, including the development of new numerical simulation tools and original experimental setups.
Fundamental studies (experimental and numerical developments, metallurgical mechanism analysis) will provide new or better knowledge which will applied in other studies in direct connection with industrial issues (support for optimizing new processes and for processing of new alloys).
In the long run, the output of the project will be applicable to types of alloys (Ti base, Al base, steels) used in aeronautics, but also in other fields like transportation or energy.

Project coordination

Nathalie Bozzolo (CEMEF MINES ParisTech)

The author of this summary is the project coordinator, who is responsible for the content of this summary. The ANR declines any responsibility as for its contents.

Partner

CEMEF CEMEF MINES ParisTech
Pprime Institut Pprime UPR 3346 ENSMA CNRS - Université de Poitiers

Help of the ANR 899,912 euros
Beginning and duration of the scientific project: December 2014 - 48 Months

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