MATETPRO - Matériaux et Procédés pour des Produits Performants

Natural Fibres Optimized Decohesion using Extrusion – DEFIBREX

Optimised Decohesion of natural Fibers using Extrusion

Numerous collaboratives actions have focused on the fiber itself : its preparation, its impact on the composite material or on such or such applications.. without undertaking the decohesion process, key factor in the compounding process. Mastering the decohesion process is fundamental for preserving dimensions ratios which induce the mechanical reinforcement mechanism.

Defibrex project objectives

The Defibrex projects assumes its objective with methodology, which is based on the analysis of natural fibers breakage under mechanical constraints.<br />This analysis should lead in defining behavioral model capable of covering a wide range of natural fibers, variants, pre-treatment and mechanical conditions. This model will be validated by experiments covering a wide range of characteristics (fibers origin, physical and chemical treatments) with the objective to assert a generic classification of mostly used fibers.

To adress these questions, the DEFIBREX project has been split into 5 technical work packages :
Fibers will be collected and characteristics under 3 axis such as morphologic, mechanical and bio-chemical (WP 1).
The WP2 will be devoted to the phenomenology of compounding at the laboratory scale with a wide range of different fibers. The compounds characterizations will be used as input for asserting a behavior model which will be used in the WP3 centered to incorporating this model in the Twin-Screw simulation software LUDOVIC® (commercial software).
The WP4 is centered on the industrial scale : fibers feeding issues, samples elaborations, compounds characterization, to widen the applications ranges and validate the behavioral model. As an additional work, the WP4 will produce the quantity of compounds required for injection of real parts. The WP5 will conduct intensive performances tests on these part to evaluate the functionality increase.

Taking into account the technical and scientific context, 4 major breakthrough have been identified : They contribute to the scientific scheme of the project, but even more they provide indeed understanding of the industrial control of all the process : They are :

. A behavioral decohesion model of natural fibers under mechanical constraints in the frame of a generic approach, with the target of incorporating the model in the TSE simulation software LUDOVIC.
. A long fibers specific feeding equipment. These types of fibers have an apparent low density which is tricky for manipulation within current industrial feeders.
. A natural fibers morphologic analysis methodology . L/D ratios is widely used and considered as the natural criterion. The DEFIBREX project proposes to provide extended criterions such as the ones available with the µtomography technique.
. An optimization of the twin screw extruders which is a complex equipment to set due to the thermal mechanical coupling occurring in the system and the validation of the twin-screw extruder for compounding natural fibers for the automotive applications.

the mid term scientific and industrials perspectives of DEFIBREX projects are of different types :
. Scientific publications on different topics such as bio material, numerical modeling, process simulation …
. Definition of natural fibers preparation methods
. Dissemination of Ludovic Software with a widen application range
. Marketing of feeding equipment dedicated to long natural fibers additives
. Production of compounds for auto motives applications
. Increase of Twin-Screw Extruders applications ranges

to be defined

All the industry from the Polymers Area, change their sourcing strategy due to 2 constraints : fossils resources availability which are the basis of the « regular » Polymers and the incentives in the reduction of the energy consumption.
This double motivation drive the car makers R&D Departments and their suppliers to evaluate and use natural fibers reinforcement as an answer to this double objective : their length is by itself a powerful mechanical reinforcement media which also leads to a very interesting density decrease. Also their natural sourcing decrease the fossil resources needs.

A great number of R&D collaboratives actions made this challenge happen focusing on the application, the fiber itself as raw material, its preparation, on the characteristics of the fibers based composite for such or such application even on the supply chain, but without accounting on the decohesion phenomena. This is a key step in the compounding stage. Mastering decohesion is important to keep fibers length which is their main attribute as mechanical reinforcement additives.
The DEFIBREX project focus on this topic with an ambitious and generic methodology, centered of the natural fibers decohesion phenomena analysis under mechanical constraints. This analysis must lead to a decohesion behavioral model which should be capable to describe a wide types of fibers and mechanical constraints ranges. This model will be validated by experiments run on a variety of fibers.( sourcing, physico-chemical treatments...) with the ambition of proposing the widest global classification of the various used fibers in the industry.
To reach these ambitious objectives, the DEFIBREX partnership associate complementary scientific skills (sourcing, pre-treatment with FRD and INRA, process and modelisation with CEMEF and µTomography morphologic analysis (I2M) , with industrial partners (K-TRON, SCC, CLEXTRAL et FAURECIA,) whose contribution will be to help reaching the project objectives and answering questions such as : how to feed a twin-screw extruder without degrading fibers length ? How to set a twin-screw extruder in such a way to maximize mixing efficiency and without degrading fibers length ? What is the functionality increase that can be expected on such injected pieces, and what is the dimensional saving that we can account ? How to deliver and disseminate the behavioral model to industrials users ?
To answer those questions, the DEFIBREX project is self organised in 5 work packages :
Fibers will be sourced and analyzed on the morphological, mechanical and bio-chemical point of view in WP1.
WP2 is dedicated to phenomenological study of the compounding process on a lab scale level with a wide range of fibers types. The compound characterization process by these experiments will be used as input for WP3 whose objective will be to set the behavioral model and its declination as a numerical model in the Twin-Screw extruder simulation program LUDOVIC (as a media for dissemination). In parallel, a fibers classification will be be proposed to establish and sort their polymers reinforcement capability, as well as the compound processability evaluation.
The WP 4 is focusing on the industrial scale : fibers feeding, productions of composites samples, compound characterization in order to wider the application range of the behavioral model. Also, the WP4 will produce compound to inject real automobile parts with the objective to evaluate the performance increase of such new parts. This will be achieved in the WP5.
Classically, the WP6 will be the project coordination work package.
Finally, DEFIBREX is expected to contribute to the knowledge and understanding of the natural fibers decohesion phenomenum and delivering to the manufacturing industry a key technological breaktrough.

Project coordination

Johnny BEAUGRAND (INRA-FARE Fractionnement des Agroressources et Environnement) – Johnny.Beaugrand@reims.inra.fr

The author of this summary is the project coordinator, who is responsible for the content of this summary. The ANR declines any responsibility as for its contents.

Partner

INRA INRA-FARE Fractionnement des Agroressources et Environnement
ARMINES CEMEF ARMINES Centre CEMEF de Mines Paris Tech
I2M Institut de Mécanique et d'Ingénierie de Bordeaux
FRD Fibres Recherche Développement
FAURECIA FAURECIA Interior System
CLEXTRAL CLEXTRAL
SCC Sciences Computers Consultants
K-TRON K-TRON

Help of the ANR 657,126 euros
Beginning and duration of the scientific project: January 2013 - 42 Months

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